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Large equipment

ASAP 2420 MIKROPORE ANALYSATOR

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University of Salzburg

Salzburg | Website

Open for Collaboration

Short Description

Gas adsorption according to the static-volumetric principle with six sample ports for the characterization of specific surfaces, pore systems in the nanometer range and gas-solid-body interactions in highly porous systems.

The ASAP 2420 allows for sample preparation at 12 heating ports and six simultaneous measurements for the determination of micro- and mesopore sizes, pore volumes and specific surfaces.

Contact Person

Univ.-Prof. Dr. Nicola Hüsing

Research Services

Investigations on the Structure of Nanoparticles and Mesoporous Solids

Methods & Expertise for Research Infrastructure

The gas adsorption analysis with nitrogen, argon, krypton or other gases allows the determination of specific surfaces and pore size distributions. With the ASAP2420 the physisorption isotherm of gas molecules on surfaces of porous solids can be fully determined under isothermal conditions (77 K for N2).

From the amount of adsorbed molecules as a function of the pressure p / p0, information about different models (BET, BJH, DFT, etc.), the specific surface area, pore size and size distribution, pore shape and surface properties (hydrophobic or hydrophilic) can be obtained.

At the University of Salzburg, pore and surface analyzes of porous solids or nanoparticulate solids, as powders or in monolithic form (metal powders, ceramic materials, catalysts, fillers, building materials, pigments, and many other solids) can be carried out.

Allocation to research infrastructure

Functional materials

Terms of Use

Please contact the University of Salzburg (science_plus@plus.ac.at) or the responsible contact person for this section mentioned in the contact field.

Cooperation Partners

Department of Geography and Geology, University of Salzburg
Department of Molecular Biology, University of Salzburg
Various industrial partners
TU Hamburg-Harburg
Vienna University of Technology
University of Vienna
Montanuniversität Leoben

Reference Projects

AB 97 Technologie und Forschungsplattform "Hybrid Materials": TFP-HyMat
2016-2018
Musso M., Hüsing N.
Interreg Österreich-Bayern 2014-2020
http://www.interreg-bayaut.net/projekte/liste-der-vorhaben/projektzusammenfassung-tfp-hymat/

Synthese, Charakterisierung und technologische Fertigungsansätze für den Leichtbau 'n2m' (nano-to-macro)
2015-2018
Hüsing, N.; Diwald, O.; Musso, M.; Bourret, G.; Redhammer, G.; Huber, O.; Saage, H.
Interreg Österreich-Bayern 2014- 2020
http://www.interreg-bayaut.net/projekte/liste-der-vorhaben/projektzusammenfassung-ab29/

Vapor phase synthesized MgO nanocubes as seed structures in solution
2015-2016
Diwald, O.
DFG
http://gepris.dfg.de/gepris/projekt/215441693

Deformation of hierarchical and anisotropic porous solids by fluid adsorption
2014-2017
Hüsing, N.; Paris, O. (Montanuniversität Leoben), Reichenauer, G. (ZAE Bayern)
FWF, DFG
http://fodok.uni-salzburg.at/pls/portal/nav.show?x=&format=full_projekt&object=75237&lang=158

Oxidische Nanostrukturen
2013-2016
Diwald, O.
DFG
http://gepris.dfg.de/gepris/projekt/238350812

Novel Pt-poor catalysts for the electrocatalytic O2 reduction based on modified, nanostructured metal oxides
2013-2016
Hüsing N., Behm R.J.
FWF/DFG


Hybrid Supercaps
2015-2018
Hüsing, N.; Paris. O.
FFG Energieforschung/ 848808


Salzburg Center for Smart Materials
2018-2022
Hüsing, N.; Tscheligi M.; Petutschnig, A.
Europäische Union/ Land Salzburg
Salzburg Center for Smart Materials - hci.plus


Monolithic Carbon Spherogels for Electrochemical Applications
2022-2025
Elsaesser, M.S., Presser, V.
FWF/DFG


Field-Enhanced Photocatalysis at Nanoscale Gaps
2020-2024
Bourret, G.; O. Diwald
FWF


Optimizing Catalyst Loading Within Nanostructured Silicon Photoelectrodes
2020-2023
Bourret, G.; Farhadi, A.
ÖAW


Charge separation within graded metal oxide nanocomposites
2023-2026
Diwald, O.; Bourret, G.
FWF

Reference Publications

Defect and Surface Area Control in Hydrothermally Synthesized LiMn0.8Fe0.2PO4 Using a Phosphate Based Structure Directing Agent
2015
Schoiber, J.; Tippelt, G.; Redhammer, G.J.; Yada, C.; Dolotko, O.; Berger, R.J.F., Husing, N.
CRYSTAL GROWTH & DESIGN Volume: 15(9), 2015, 4213-4218.
DOI: 10.1021/acs.cgd.5b00324

Ordered Meso-/Macroporous Silica and Titania Films by Breath Figure Templating in Combination with Non-Hydrolytic Sol-Gel Processing
2015
Feinle, A.; Akbarzadeh, J.; Peterlik, H.; Hüsing, N.
Microporous and Mesoporous Materials
doi:10.1016/j.micromeso.2015.06.043


A Two-Step Synthesis for Li2CoPO4F as High-Voltage Cathode Material
2015
Schoiber, J.; Berger, R.J.F.; Yada, C.; Miki, H.; Husing, N.
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
DOI: 10.1149/2.0331514jes

Self-supporting hierarchically organized silicon networks via magnesiothermic reduction
2016
Waitzinger, M.; Elsässer, M.S.; Berger, R.J.F.; Akbarzadeh, J.; Peterlik, H.; Hüsing, N.
MONATSHEFTE FÜR CHEMIE
DOI:10.1007/s00706-015-1611-8


Sol-gel synthesis of monolithic materials with hierarchical porosity
2016
Feinle, A.; Elsässer, M.E.; Hüsing, N.
Chem. Soc. Rev.
DOI:10.1039/c5cs00710k


Chemical phase separation strategies towards silica monoliths with hierarchical porosity
2013
Triantafillidis, C.; Elsässer, M.E.; Hüsing, N.
Chem. Soc. Rev. Vol.: 42 Pages: 3833-3846
DOI:10.1039/C3CS35345A

High Surface Area Crystalline Titanium Dioxide: Potential and Limits in Electrochemical Energy Storage and Catalysis
2012
Fröschl, T.; Hörmann, U.; Kubiak, P.; Kucerova, G.; Pfanzelt, M.; Weiss, C.K.; Behm, R.J.; Hüsing, N.; Kaiser, U.; Landfester, K.; Wohlfahrt-Mehrens, M.
Chem. Soc. Rev. Vol.: 41 Pages: 5313-53,
DOI:10.1039/C2CS35013K

Reversibly compressible and freestanding monolithic carbon spherogels
2019
Miralem Salihovic, Gregor A. Zickler, Gerhard Fritz-Popovski, Maike Ulbricht, Oskar Paris, Nicola Hüsing, Volker Presser, Michael S. Elsaesser
Carbon
https://www.sciencedirect.com/science/article/pii/S0008622319306621


Monolithic Spiropyran-Based Porous Polysilsesquioxanes with Stimulus-Responsive Properties
2020
Daniel Euchler, Caroline R. Ehgartner, Nicola Hüsing, Andrea Feinle
ACS Appl. Mater. & Interf.
https://pubs.acs.org/doi/10.1021/acsami.0c14987


Monolithic Carbon Spherogels as Freestanding Electrodes for Supercapacitors
2021
Miralem Salihovic, Philipp Schlee, Servann Herou, Maria-Magdalena Titirici, Nicola Hüsing, Michael S. Elsaesser
ACS Applied Energy Materials
https://pubs.acs.org/doi/full/10.1021/acsaem.1c02055


A facile one-pot synthesis towards hierarchically organized Carbon/TiO2 monoliths with ordered mesopores
2021
Jürgen Schoiber, Christian Koczwara, Simon Rumswinkel, Laurence Whitmore, Christian Prehal, Florian. Putz, Michael S. Elsaesser, Oskar Paris, Nicola Hüsing
ChemPlusChem
https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/cplu.202000740


Renewable, Organic and Related Carbon Aerogel Monoliths from the Polycondensation of Tannin with 5-(Hydroxymethyl)furfural
2022
Ann-Kathrin Koopmann,Theresa Bartschmid, Nicola Hüsing, Michael S. Elsaesser
Journal of Sol-Gel Science and Technology
https://link.springer.com/article/10.1007/s10971-022-06015-4


Black goes green: single-step solvent exchange for sol-gel synthesis of carbon spherogels as high-performance supercapacitor electrodes
2024
Miralem Salihovic, Emmanuel Pamete´, Stefanie Arnold, Irena Sulejmani, Theresa Bartschmid, Nicola Hu¨sing, Gerhard Fritz-Popovski, Chaochao Dun, Jeffrey J. Urban, Volker Presser, M. S. Elsaesser
RSC Energy Advances
https://pubs.rsc.org/en/content/articlehtml/2024/ya/d3ya00480e


Sustainable Tannin Gels for the Efficient Removal of Metal Ions and Organic Dyes
2023
A.K. Koopmann, C.R. Ehgartner, D. Euchler, M. Claros, N. Huesing
Gels
https://doi.org/10.3390/gels9100822


Charge Separation in BaTiO3 Nanocrystals: Spontaneous Polarization Versus Point Defect Chemistry
2023
E Neige, T Schwab, M Musso, T Berger, GR Bourret, O Diwald
Small
https://onlinelibrary.wiley.com/doi/full/10.1002/smll.202206805
e2206805

Contact

Univ.-Prof. Dr. Nicola Hüsing
Fachbereich Chemie und Physik der Materialien
+43-662-8044-6265
nicola.huesing@plus.ac.at
https://www.plus.ac.at/chemie-und-physik-der-materialien/

Location

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